Study on Heat Treatment Process of ASTM A565 XM-32 Stainless Steel
11 July 2025 9 Blog

Study on Heat Treatment Process of ASTM A565 XM-32 Stainless Steel

Dr. Robert Anderson

Dr. Robert Anderson

Senior Materials Scientist

Abstract

This study investigates the effect of heat treatment processes on the mechanical properties of ASTM A565 XM-32 stainless steel at room temperature. The results show that when the quenching temperature is 1030°C, the tensile strength and impact toughness reach their peak values. However, the tempering holding time should not be excessively prolonged.

Keywords: ASTM A565 XM-32, quenching temperature, tempering time

Introduction

ASTM A565 XM-32 stainless steel is used for manufacturing turbine wheels in gas turbines. Due to the demanding working environment, the steel must exhibit high strength and impact toughness at room temperature (A_k ≥ 100 J, as per ASTM A565 standards). Additionally, it must withstand a specified temperature (595°C) and load (240 MPa) for 30 hours without fracture in notched composite specimens. To ensure the success of the heat treatment process and avoid repeated treatments, a series of experiments were conducted to determine the optimal parameters.

Technical Requirements

1. Chemical Composition

The chemical composition requirements (mass fraction, %) are listed in Table 1.

Table 1: Chemical composition requirements

C Mn Si Ni Cr Mo V P S N
0.08–0.15 ≤0.90 ≤0.30 2.50–3.00 11.50–12.25 1.50–2.00 0.25–0.40 ≤0.015 ≤0.010 ≤0.06

Residual elements: Al ≤ 0.05%, As ≤ 0.15%, Sn ≤ 0.10%, Sb ≤ 0.003%.

2. Mechanical Properties at Room Temperature

The mechanical property requirements are listed in Table 2.

Table 2: Mechanical property requirements

R_m (MPa) R_p (MPa) A (%) Z (%) A_k (J) HB
≥830 ≥1035 ≥13 ≥30 ≥100 321–352

Experimental Procedure

1. Material Preparation

The steel was produced using the EAF + LHF + VCD + ESR process. The melting analysis is shown in Table 3.

Table 3: Melting analysis (mass fraction, %)

C Mn Si Ni Cr Mo V P S N Cr_eq
0.12 0.76 0.18 2.76 11.81 1.7 0.31 0.012 0.001 0.03 4.8

2. Forging and Processing

  • Forging temperature: 880°C–1180°C.
  • Samples were forged into Φ60 mm billets and then machined into Φ30 mm specimens.

3. Heat Treatment Schemes

Five heat treatment schemes were tested:

  1. Quenching at 990°C (1 h, oil cooling), tempering at 560°C (3 h, oil cooling).
  2. Quenching at 1010°C (1 h, oil cooling), tempering at 560°C (3 h, oil cooling).
  3. Quenching at 1030°C (1 h, oil cooling), tempering at 560°C (3 h, oil cooling).
  4. Quenching at 1040°C (1 h, oil cooling), tempering at 560°C (3 h, oil cooling).
  5. Quenching at 1050°C (1 h, oil cooling), tempering at 560°C (3 h, oil cooling).

Results and Discussion

  1. Effect of Quenching Temperature:

    • At 1030°C, tensile strength and impact toughness peaked.
    • Higher temperatures (>1030°C) led to grain coarsening, reducing strength and toughness.
  2. Effect of Tempering Time:

    • Extending tempering time to 5 hours caused carbides to coarsen, reducing strength and toughness.

Conclusion

  1. The optimal quenching temperature for ASTM A565 XM-32 is 1030°C.
  2. Tempering time should not exceed 3 hours to avoid performance degradation.
  3. The recommended heat treatment process is:
    • Quenching: 1030°C for 1 hour, oil cooling.
    • Tempering: 580°C for 3 hours, oil cooling.

References

  1. Tanaka, T. Ferritic Stainless Steels. Translated by Zhang Jiayuan, Zhang Shaolin. Beijing: Metallurgical Industry Press, 2003.
  2. China Materials Engineering Canon (Vol. 3): Iron and Steel Materials Engineering (Part 2). Beijing: Chemical Industry Press, 2005.
  3. Cui Zhiwu, Cao Zhenchun. Metallurgy and Heat Treatment, 2nd Edition. Beijing: Mechanical Industry Press, 2007.

SEO Optimization Notes:

  • Title: Includes key terms like "ASTM A565 XM-32" and "heat treatment" for searchability.
  • Keywords: Highlighted for SEO.
  • Structured Content: Clear sections (Abstract, Introduction, Results, Conclusion) improve readability and indexing.
  • Technical Details: Tables and specific parameters enhance relevance for technical searches.
  • Citations: References add credibility and depth.

FAQ